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Oxidation resistance of pressureless-sintered SiC-AlN-Re2O 3 composites Obtained without powder bed

TitoloOxidation resistance of pressureless-sintered SiC-AlN-Re2O 3 composites Obtained without powder bed
Tipo di pubblicazionePresentazione a Congresso
Anno di Pubblicazione2009
AutoriMagnani, G., Antolini F., Beaulardi L., Burgio F., and Mingazzini C.
Conference NameCeramic Engineering and Science Proceedings
Conference LocationDaytona Beach, FL
Parole chiaveAlN, Alumina, Ceramic materials, Corrosion, Corrosion fatigue, Cost-effective methods, Grain boundaries, Grain-boundary phasis, Interfacial reactions, Lutetia, oxidation, Oxidation behaviours, Oxidation resistance, Oxygen, Powder beds, Powders, Pressureless-sintered, Rare earth elements, Rare-earth oxides, Rate-determining steps, Silica, Silica aluminas, Silicon carbide, Sintered alumina, Sintered densities, Sintered samples, Sintering, Solid solutions, Surface diffusion, Surface reactions, Temperature ranges, Well-dispersed
Abstract

Oxidation resistance of SiC-AlN-Re2O3 composites (SiC 50%wt-AlN 50%wt) pressureless-sintered with an innovative and cost-effective method is reported, Yttria, Lutetia, Ytterbia and Erbia were tested as sintering-aids in this pressureless-sintered process which does not require the use of the powder bed to protect samples during the heat treatments, Sintered density was always >95%T.D. and microstructure was mainly composed by 2H SiC-AlN solid solution with well-dispersed grain boundary phases. The sintered samples, after oxidation in the temperature range 1200-1200°C over a period of time of 200h, showed a parabolic oxidation behaviour with diffusion of oxygen through the silica-based surface and interfacial reactions silica-alumina and silica-rare-earth oxides as rate-determining steps.

URLhttps://www.scopus.com/inward/record.uri?eid=2-s2.0-62849096844&partnerID=40&md5=7fd68c13031510d9a52115a20eb8e279
Citation KeyMagnani200921